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Project Report · Bioreactor Series · Arthrospira platensis

Spirulina Liquid Air Purifier
— Liquid Tree Design

Complete technical guide: Zarrouk's Medium recipe, CO₂/O₂ exchange data, LED lighting protocol, preservation strategy, maintenance schedule, and a full troubleshooting guide.

Arthrospira platensis Zarrouk Medium (1966) CO₂ → O₂ Conversion Photobioreactor DIY & Lab Grade Liquid Tree Design
// Contents
  1. Overview — What & Why Liquid Tree?
  2. Spirulina Culture Medium — Full Recipe (1 Liter)
  3. Step-by-Step Preparation Protocol
  4. How to Operate Your Bioreactor
  5. How to Preserve the Culture
  6. CO₂ Consumption & O₂ Production Data
  7. LED Light Cycle — Type & Schedule
  8. Maintenance Schedule (Daily / Weekly / Monthly)
  9. Troubleshooting Quick Guide

01 Overview — What & Why Liquid Tree?

A Liquid Tree is a photobioreactor filled with live spirulina culture. The spirulina (Arthrospira platensis) performs photosynthesis under LED light, absorbing CO₂ from pumped-in room air and releasing O₂ — exactly like a tree, but in liquid form and 10–50× more efficient per unit of space.

The concept was publicly demonstrated in Belgrade, Serbia, where 600-litre street-side Liquid Tree installations replaced benches and trees in high-pollution zones. The same biology scales down to a 1-litre desktop unit that can meaningfully contribute to air quality in a room.

// Photosynthesis Equation 6 CO₂ + 6 H₂O + light energy → C₆H₁₂O₆ (biomass) + 6 O₂

Spirulina is 10–50× more photosynthetically efficient per square metre than a land tree. It also removes NOₓ and SOₓ from the air as nitrogen and sulphur nutrients. 1 kg of dry spirulina biomass locks up 1.83 kg of CO₂ permanently.

The liquid medium (Zarrouk's Medium, 1966) provides all nutrients spirulina needs to grow, photosynthesize, and remain healthy long-term. The sections below give you the complete recipe, protocol, and operational guide.

02 Spirulina Culture Medium — Full Recipe (1 Liter)

The industry standard is Zarrouk's Medium (1966), used globally for Arthrospira platensis cultivation. It is prepared as two separate solutions to prevent mineral precipitation before autoclaving, then combined aseptically.

Solution A — 500 mL of the final 1 L

#Chemical NameFormulaAmount per 1 L finalRole
1Sodium BicarbonateNaHCO₃16.80 gPrimary carbon source & pH buffer (alkaline ~9.5–10.5)
2Dipotassium Hydrogen PhosphateK₂HPO₄0.50 gPhosphorus source for cell growth & energy transfer

Solution B — 500 mL of the final 1 L

#Chemical NameFormulaAmount per 1 L finalRole
3Sodium NitrateNaNO₃2.50 gPrimary nitrogen source for protein & pigment synthesis
4Potassium SulfateK₂SO₄1.00 gPotassium & sulfur supply
5Sodium ChlorideNaCl1.00 gOsmotic balance
6Magnesium Sulfate HeptahydrateMgSO₄·7H₂O0.20 gMagnesium — essential for chlorophyll production
7Calcium Chloride DihydrateCaCl₂·2H₂O0.04 gCalcium for cell wall structure
8Iron(II) Sulfate HeptahydrateFeSO₄·7H₂O0.01 gIron for photosynthesis enzymes (ferredoxin)
9Disodium EDTA DihydrateEDTA-Na₂·2H₂O0.08 gChelator — keeps iron & metals bioavailable to cells

Solution C — Micronutrient Stock (add 10 mL per final 1 L of culture)

Prepare 1 litre of this stock separately. Store in 10 mL aliquots frozen. Add 10 mL to each litre of finished culture.

ChemicalFormulaAmount in Stock (per 1 L stock solution)Role
Boric AcidH₃BO₃2.86 gBoron — cell wall integrity & pollen tube growth
Manganese Chloride TetrahydrateMnCl₂·4H₂O1.81 gManganese — oxygen evolution in photosynthesis
Zinc Sulfate HeptahydrateZnSO₄·7H₂O0.222 gZinc — enzyme cofactor (carbonic anhydrase)
Copper Sulfate PentahydrateCuSO₄·5H₂O0.079 gCopper — electron transport (plastocyanin)
Molybdenum TrioxideMoO₃0.015 gMolybdenum — nitrogen fixation & nitrate reductase
// Water Quality Warning Always use distilled or de-chlorinated water. Tap water chlorine kills the culture. Use a Brita/activated carbon filter or leave tap water uncovered for 24 hours before use to off-gas chlorine.

Target Parameters After Mixing

9.5pH minimumMinimum acceptable
10.0pH optimalBest growth range
10.5pH maximumUpper safe limit
30–35°CTemperatureOptimal growth range

03 Step-by-Step Preparation Protocol

// DIY Shortcut — Pre-Mixed Zarrouk Powder Commercial pre-mixed Zarrouk powder is available (Phydrotec, HealthAlgae). Simply weigh 22 g of powder and dissolve in 1 L of de-chlorinated water. This eliminates the multi-step process and is accurate for home and small-scale Liquid Tree builds.

04 How to Operate Your Bioreactor

The spirulina liquid medium functions as the living engine of your air purifier. Here is the complete operational procedure:

Starting the Culture

Daily Operation

Run the air pump continuously or at minimum 18 hours/day (in sync with lights). The spirulina absorbs CO₂ from the air bubbles and releases O₂. Normal room air (0.04% CO₂) is sufficient for a small unit, though supplementing with 2–5% CO₂ greatly increases output.

// Optimal Spirulina Culture Density Target 400–600 mg dry weight per litre. Below 100 mg/L the culture is too thin and cells experience photoinhibition. Above 1,500 mg/L, cells self-shade and growth slows dramatically. Monitor by color: deep emerald green = healthy; olive/yellow = stressed; brown = dying.

05 How to Preserve the Culture

Short-Term (Days to Weeks)

Keep the live culture in medium at 25–30°C with reduced lighting (8 hours/day, dimmer) and gentle aeration. Replenish evaporated water with distilled water every 2–3 days. The culture stays active and healthy for several weeks with minimal maintenance.

Medium-Term (Weeks to 3 Months) — Dormancy Mode

Place a small sample (100 mL) in fresh medium, reduce light to 4 hours/day, and lower temperature to 15–20°C. The culture enters slow dormancy. Add a small amount of urea (0.01 g/L) and iron chelate once a month to maintain viability. Reactivate by gradually increasing light, temperature, and nutrients over 3–5 days.

Long-Term Backup (Months to Years)

For laboratory-grade preservation: cryopreservation in 10% DMSO at −80°C. For home use, maintaining a small 100 mL "mother culture" on a windowsill with occasional nutrient top-ups is the most practical backup strategy. Keep it in a sealed glass jar away from harsh direct sunlight.

Preserving Prepared Medium Without Spirulina

Sterile Zarrouk medium (without spirulina inoculated) can be stored in a sealed glass container at 4°C (refrigerator) for up to 3 months without degradation. Label with preparation date.

// Culture Collapse Warning Signs — Act Immediately Yellowish color = nitrogen depletion or pH drift. Foamy + yellow = cell lysis (dead culture). Brown color = temperature shock or contamination. In all cases: remove 50–80% of culture, replace with fresh Zarrouk medium and fresh starter inoculum.

06 CO₂ Consumption & O₂ Production Data

These figures are sourced from peer-reviewed bioreactor studies of Arthrospira platensis under controlled conditions.

25.1g CO₂ / m³ / hourPeak CO₂ fixation rate at 2.5% CO₂ input, 150 µmol m⁻² s⁻¹, 25°C
1.83kg CO₂ per kg dry biomassMass ratio consumed during growth
99%CO₂ removal efficiencyAt 2.5% CO₂ input, 25°C, optimal light
~1.5×O₂ producedMass ratio vs CO₂ consumed (photosynthesis stoichiometry)

Practical Estimate for a 1-Litre Bioreactor

ConditionCO₂ Consumed / dayO₂ Produced / dayNotes
Low — dim light, ambient CO₂~0.025 g~0.018 gRoom air only, 12h light cycle
Medium — good LED, ambient CO₂~0.1–0.5 g~0.07–0.4 g16h LED, aerated, ~500 mg/L density
High — 2.5% CO₂ injection~0.6 g~0.45 gActive CO₂ enrichment, optimal temperature
// Scale Context: When Does It Equal a Tree? A healthy adult tree absorbs roughly 21 kg CO₂/year (~57 g/day). A 1-litre spirulina bioreactor under good conditions absorbs 0.1–0.6 g/day — at vastly higher efficiency per unit volume. Scale to 200 litres and it begins approaching a real tree. The Belgrade street Liquid Tree installations run at 600-litre scale — which is why they work as genuine urban air purifiers.

Night / Dark Period Behaviour

Spirulina stops photosynthesis in darkness and shifts to cellular respiration, which slightly reverses the process — consuming a small amount of O₂ and releasing CO₂. Keep the dark period to 8 hours or less. The net 24-hour balance is still strongly positive for O₂ production.

07 LED Light Cycle — Type & Schedule

Best LED Type for Spirulina

LED TypeColor TempPerformanceRecommendation
Daylight White LED6500 KExcellent biomass & pigment production, most energy efficient✅ Best Choice
Warm White LED3000 KSimilar biomass growth, uses 4.53 kWh more per cycleGood alternative
Red + Blue Combo660 nm + 470 nmExcellent photosynthetic efficiency, higher costGood for advanced setups
Green LED only520 nmPoorest growth rate — spirulina reflects green light❌ Avoid entirely
// Why Daylight 6500K? 6500K LEDs are rich in blue wavelengths (~470 nm), which are strongly absorbed by chlorophyll-a — spirulina's primary photosynthetic pigment. They are the most energy-efficient option, consuming ~4.53 kWh less energy than warm white LEDs while producing equal or better biomass yield per cycle.

Optimal Light Intensity

Target 80–160 µmol photons m⁻² s⁻¹ (approximately 2,000–4,000 lux). For a small home bioreactor, place a 15–20W daylight LED strip 10–15 cm from the vessel surface. Too much light (>200 µmol m⁻² s⁻¹) causes photoinhibition — the spirulina shuts down its photosystems. Too little causes slow growth and thin culture.

Recommended Light/Dark Cycle — 16L : 8D

Research confirms the best balance between biomass productivity and energy efficiency is the 16:8 photoperiod:

💡 LIGHT ON — 16 hours
🌙 DARK — 8 hours

Use a simple plug-in outlet timer. For example: lights ON at 6:00 AM, lights OFF at 10:00 PM. The dark period is essential — it prevents culture stress and allows cellular repair processes.

PhotoperiodBiomass ProductivityEnergy EfficiencyNotes
12L : 12DModerateGoodMinimum for sustained healthy culture
16L : 8DHighExcellent ✅Best balance — recommended for all setups
20L : 4DVery HighGoodBest productivity, higher electricity cost
24L : 0DHigh (initially)PoorCulture stress long-term — not sustainable

08 Maintenance Schedule

Daily Tasks

TaskWhat to DoWhy
Check colorDeep emerald green = healthy. Yellow/olive = problem. Brown = emergency. Act immediately if off-color.Primary early-warning indicator
Check aerationConfirm air pump is running, bubbles are visible throughout the culture.CO₂ supply & culture mixing
Top up waterAdd a small amount of distilled water to maintain volume (evaporation loss).Prevents salt concentration increase
Light timerConfirm LED timer is working on 16:8 schedule.Consistent photoperiod

Weekly Tasks

TaskWhat to Do
pH checkMeasure pH. Should be 9.5–10.5. Adjust with a few drops of 0.1M NaOH (raise) or 0.1M HCl (lower).
TemperatureConfirm 28–35°C. Below 20°C slows growth significantly. Above 38°C is damaging to spirulina cells.
Density checkHold a sample jar to light — should be opaque green, not see-through. Aim for 400–600 mg/L dry weight.
Partial harvestRemove 10–15% of the culture volume. Replace with fresh Zarrouk medium. Keeps nutrients balanced and culture young.
Nutrient top-upAdd a small dose of NaHCO₃ (1–2 g per 1 L) if culture looks pale — bicarbonate depletes as the primary CO₂ source.

Monthly Tasks

TaskWhat to Do
Full medium refreshReplace 30–50% of culture medium with freshly prepared Zarrouk medium. Prevents salt buildup and nutrient imbalance.
Clean vesselWipe inside walls of the bioreactor with a soft cloth to remove biofilm that blocks light penetration.
Check tubing & pumpInspect air tubes for blockages, algae growth in lines, pump wear. Replace air stone if bubbling is uneven.
Backup cultureSave 50–100 mL of healthy culture in a small sealed jar in the fridge as emergency restart stock.
MicronutrientsAdd 1–2 mL of micronutrient Stock C per litre to replenish trace elements consumed by spirulina growth.
// Semi-Continuous Harvesting — The Best Long-Term Method Remove 10–15% of the culture volume every 2–3 days and replace with fresh medium. This keeps the culture in constant exponential growth phase — the state of maximum CO₂ uptake and O₂ production. It is the same method used in commercial Liquid Tree installations.

09 Troubleshooting Quick Guide

SymptomLikely CauseFix
Culture turns yellowishNitrogen depletion, pH drift, or photoinhibitionAdd NaNO₃ (0.5 g/L), check pH, reduce light intensity to 80–100 µmol m⁻² s⁻¹
Culture turns olive/brownTemperature shock (<15°C or >38°C) or contaminationRestore temperature to 30–35°C, replace 50% with fresh medium + fresh inoculum
Foamy yellow liquidCell lysis — culture is dying or deadDiscard most of it, keep 10%, inoculate into 100% fresh Zarrouk medium with fresh starter
Culture too thin (pale green)Low inoculum, nutrient depletion, or insufficient lightAdd more spirulina starter, top up with Zarrouk medium, increase light to 120–150 µmol m⁻² s⁻¹
Slow or no growthTemperature too low, pH out of range, or light incorrectOptimal: temp = 30–35°C, pH = 9.5–10.0, light = 80–160 µmol m⁻² s⁻¹. Adjust all three systematically.
White/gray residue on glassSalt precipitation (mineral deposits)Wipe clean with soft cloth. Ensure A and B solutions were mixed after autoclaving, not before.
Unpleasant smellBacterial contaminationReplace 80% with fresh medium. Ensure air inlet tube has an inline air filter (0.22 µm) to prevent bacterial entry.
// Golden Rule Always keep a backup culture. 50–100 mL of healthy spirulina in a small jar in your refrigerator can restart a completely crashed system within 7–10 days.

Optimal Conditions — Quick Reference

30–35°CTemperatureIdeal growth range
9.5–10.0pHAlkaline & stable
16 : 8Light : Dark hoursOptimal photoperiod
6500 KLED Color TempDaylight white LED
~120 µmolm⁻² s⁻¹ intensity~3,000 lux at vessel surface
400–600mg dry weight / LTarget culture density
// Sources & References
  • Zarrouk, C. (1966). Contribution à l'étude d'une cyanophycée. Université de Paris — standard medium formulation.
  • Hindawi International Journal of Biotechnology, 2013 — Zarrouk medium validation study.
  • Redalyc Journal: CO₂ biofixation rates for Spirulina platensis bioreactors.
  • OCL Journal (Oilseeds and Fats, Crops and Lipids), 2021 — LED light cycle comparison (16:8 vs 20:4 vs 12:12).
  • ScienceDirect — LED energy efficiency comparison (6500K vs 3000K) for microalgae cultivation.
  • UTEX Culture Collection — Spirulina preservation and culture protocols.
  • AACL Bioflux, 2024 — CO₂ fixation and O₂ production rates for photobioreactors.
  • Molecular Biotechnology, 2023 — Photoperiod optimisation for Arthrospira platensis.